Morphologic Analysis of Zirconia Ceramics: Effect of Different Surface Treatments.

PURPOSE: To investigate the effects of airborne-particle abrasion and nanosilica (nano-Si) infiltration treatment on the surface characteristics of dental zirconia. MATERIALS AND METHODS: A total of 15 unsintered zirconia ceramic green bodies (10 × 10 × 3 mm) were divided into three groups (n = 5): Group C, no treatment after sintering; Group S, airborne-particle abrasion with 50-µm aluminum oxide particles after sintering; and Group N, infiltration of nano-Si followed by sintering and hydrofluoric acid (HF) etching. The zirconia disks' surface roughness was analyzed by atomic force microscopy (AFM). The surface morphology of the specimens was analyzed using scanning electron microscopy (SEM), and the chemical composition was analyzed by energy-dispersive x-ray (EDX). Data were statistically analyzed by the Kruskal-Wallis test (P < .05). RESULTS: Zirconia surface treatments by infiltration of nano-Si, sintering, and HF etching showed multiple changes in the surface features. The surface roughness of Groups C, S, and N were 0.88 ± 0.07 µm, 1.26 ± 0.10 µm, and 1.69 ± 0.15 µm, respectively. The surface roughness of Group N was significantly higher than that of Groups C and S (P < .05). EDX analysis showed peaks that corresponded to silica (Si) after infiltration with colloidal Si that disappeared following acid etching. CONCLUSIONS: Infiltrating nano-Si increases the surface roughness of zirconia. The formation of retentive nanopores on the surface potentially improves the zirconia-resin cement bonding strengths.

Five-year Clinical Evaluation of Universal Adhesives in Noncarious Cervical Lesions.

OBJECTIVES: To compare the clinical performance of mildly acidic universal adhesives Scotchbond Universal (SU, 3M Oral Care, St Paul, MN, USA) and Prime & Bond Elect (PBE, Dentsply Sirona, Charlotte, NC, USA) in the restoration of noncarious cervical lesions (NCCLs). METHODS AND MATERIALS: A total of 63 patients in need of 203 NCCL restorations participated in this randomized controlled clinical trial. Notch-shaped lesions were restored with Kalore (GC Corporation, Tokyo, Japan) after application of either SU or PBE, following the etch-and-rinse (ER) or self-etch (SE) techniques. Subjects were followed up for 60 months. The focus of the statistical analyses was on the change of outcome over time as assessed by the Modified USPHS rating system (ie, Alfa vs Bravo + Charlie outcomes). Logistic regression was performed for each outcome separately with compound symmetric variance-covariance structure assumed to consider a correlation of restorations within subjects. All analyses were conducted using SAS 9.4 (SAS, Cary, NC, USA). RESULTS: One-hundred twenty-nine teeth in 35 subjects were assessed at the 60-month follow-up. In addition, three restorations that failed prior to the 60-month evaluation, two of which were in subjects who did not present for the 60-month follow-up, were included in the statistical analysis. In total, two restorations in the SU_ER group and three restorations in the PBE_SE group failed the retention category. Statistically significant differences were obtained for the comparison of restorations in the PBE_SE and PBE_ER groups, where the former was 58% less likely to maintain a score of Alfa for marginal discoloration than the latter. CONCLUSIONS: SU and PBE demonstrated acceptable clinical performance at 60 months with regard to restoration retention. Phosphoric-acid etching of the NCCLs prior to adhesive application significantly improved the performance of PBE in regard to marginal discoloration.

Efficacy of adhesive strategies for restorative dentistry: A systematic review and network meta-analysis of double-blind randomized controlled trials over 12 months of follow-up.

PURPOSE: The efficacy of etch-and-rinse, selective enamel-etching, and self-etching protocols for universal adhesives in follow-ups of over 12 months was compared in a network meta-analysis. STUDY SELECTION: Randomized controlled trials (RCTs) published from 1998 to 2022 that compared marginal staining, marginal adaptation, retention and fractures, post-operative sensitivity, or recurrence of caries that took place over 12-months post-restoration were selected. A network meta-analysis determined the performance of each adhesive protocol. RESULTS: After screening 981 articles, 16 RCTs were subjected to data extraction. Of which, 674 patients with 2816 restorations, were included in the network meta-analysis. The pooled risk of marginal discoloration following self-etching was significantly higher than that following etch-and-rinse at over 12, 24, and 36 months, which was time-dependent. The pooled risks of unfavorable marginal adaptation and unfavorable retention and fractures following self-etching were also significantly higher than that following etch-and-rinse, with the rates of unfavorable retention and fractures in non-carious cervical lesions increasing in a time-dependent manner. The pooled risks of marginal discoloration, unfavorable marginal adaptation, retention and fractures were similar between etch-and-rinse and selective enamel-etching protocols. Post-operative hypersensitivity and recurrence of caries were not significantly different among etch-and-rinse, selective enamel-etching, and self-etching protocols. CONCLUSIONS: In follow-ups over 12 months, esthetic and functional outcomes of restorations completed with an etch-and-rinse adhesive protocol were superior to the ones achieved with a self-etching strategy without selective enamel-etching. Selective enamel etching is recommended for self-etching systems. Biological responses were similar for all three adhesive strategies.

Shear bond strength of metallic orthodontic brackets to zirconium crowns treated by sandblasting compared to enamel using a universal adhesive: An in vitro study.

OBJECTIVES: Orthodontic brackets are increasingly bonded to the surface of zirconium crowns due to the growing aesthetic demands in adults' restorations. Therefore, providing a reliable bond between these substrates is of great importance. This study aimed at investigating the shear bond strength (SBS) of orthodontic metal brackets bonded to zirconium treated by sandblasting. In addition, the value was compared with SBS between metal brackets and enamel. MATERIALS AND METHODS: Samples were divided into three groups including first premolar enamel specimens (n=20), untreated zirconium blocks (n=20) and sandblasted zirconium blocks (n=20). Enamel specimens underwent etching and bonding procedures using 37% phosphoric acid and 3M™ Scotchbond™ Universal adhesive. Zirconium blocks were randomly allocated to two groups. The first group was prepared by sandblasting with 50µm aluminium oxide particles (Al2O3) under 4 bars pressure followed by bonding brackets with 3M™ Scotchbond™ Universal adhesive. Metal brackets were also bonded to the untreated zirconium group using the same adhesive. All samples underwent thermocycling, and SBS was calculated using a universal testing machine with a crosshead speed of 1mm/min. Data were analysed using One-way Anova and Tukey's tests. RESULTS: The highest SBS was recorded in sandblasted zirconium group (26.17±8.22MPa) followed by enamel group (23.667±7.00MPa) and untreated zirconium group (11.49±7.00MPa). There was a significant difference between the SBS of untreated zirconium and that of two other groups. CONCLUSION: Perfect SBS was achieved by sandblasting pre-treatment, comparable to that of enamel. Therefore, sandblasting of zirconium crowns is recommended prior to bonding orthodontic brackets.

Comparative Study of Chemical and Mechanical Surface Treatment Effects on The Shear Bond Strength of Polyether-Ether-Ketone to Veneering Resin.

PURPOSE: To assess the shear bond strength of composite resin to polyether ether ketone (PEEK) after mechanical and chemical surface treatments. MATERIALS AND METHODS: A total of 48 PEEK discs were fabricated and divided equally into four surface treatment groups (n = 12 each): (1) airborne particle abrasion with 50-µm alumina particles at 2 MPa pressure for 10 seconds; (2) 98% sulfuric acid etching for 1 minute; (3) airborne particle abrasion and sulfuric acid etching; and (4) no surface treatment. Specimens were conditioned, then Gradia composite veneer (GC) was applied to the PEEK surfaces and polymerized. Bond strength was measured with shear bond test using a universal testing machine. One-way analysis of variance and Tukey post hoc tests were applied for statistical analysis. RESULTS: The mean shear bond strength values of the sulfuric acid-etched group were higher than that of the airborne particle abrasion + acid etching, airborne particle abrasion, and control groups (P < .05). Mean shear bond strength values for the airborne particle abrasion + acid etching samples were higher than for the control and airborne particle abrasion groups (P < .05). CONCLUSION: There was no significant difference between the samples treated with airborne particle abrasion and the control group.

Effect of surface treatment and manufacturing process on the shear bond strength of veneering composite resin to polyetherketoneketone (PEKK) and polyetheretherketone (PEEK).

STATEMENT OF PROBLEM: Polyaryletherketones (PAEKs) are high-performance polymer materials in which polyetheretherketone (PEEK) and polyetherketoneketone (PEKK) are the most used. Although mechanical and shear bonding strength tests have been performed on the 2 materials, studies on the influence of processing on bonding are scarce. PURPOSE: The purpose of this in vitro study was to determine the influence of the surface treatment and the manufacturing process on the shear bond strength of veneering composite resin to PEKK and PEEK. MATERIAL AND METHODS: Thirty pressed PEKK, 30 milled PEKK, and 30 milled PEEK specimens were distributed in 6 groups (n=13) as per the manufacturing process and treatment surface. The specimens were either treated with airborne-particle abrasion with 110-µm aluminum oxide, or no surface treatment was applied. Moreover, the PEKK specimens were grouped regarding their manufacturing process, as either milled or heat-pressed. The specimens were all bonded by using a methyl methacrylate-based adhesive (visio.link), and composite resin (Gradia Revolution 2) was bonded to the specimens. An Instron universal machine was used to calculate the shear bond strength between the PEEK or PEKK and the composite resin. Two specimens from each group had their topography modification assessed with a scanning electron microscope. Statistical analysis was performed by using a 3-way ANOVA for multiple comparisons (α=0.05) RESULTS: The groups that were surface treated with 110-µm aluminum oxide (Al2O3) before bonding showed significantly higher shear bond strength (P=.001) than the other groups. However, no statistically significant difference was observed among the groups, regardless of the manufacturing process (milled or heat-pressed) (P=.607). CONCLUSIONS: PEEK and PEKK surfaces treated with 110-µm aluminum oxide airborne-particle abrasion displayed better shear bond strength to composite resin. The manufacturing process (milled or heat-pressed) did not significantly affect the bond strength of PEKK when subjected to the same bonding process.

Pre-cementation procedures' effect on dental zirconias with different yttria content.

OBJECTVE: Several pre-cementation procedures have been advocated to enhance adhesion between zirconia and resin-based cement. There is, however, limited documentation on how these pre-treatments affect the strength of zirconia crowns as most tests are performed on discs or bars. The aim was to assess the effect of pre-cementation procedures on fracture mode, fracture strength and cement retention on zirconia. METHODS: Two dental zirconia materials with different yttria content were assessed (<4 and>5 mol%). Both discs (n = 45) and crown-shaped specimens (n = 30) of the two materials were pretreated with either air-abrasion or hot-etching with KHF2 and compared with untreated controls with regards to surface roughness, crystallography, wettability, cement adhesion and fracture strength. RESULTS AND SIGNIFICANCE: Air-abrasion improves adhesion and strength of zirconia with moderate yttria content (<4 mol%). Acid etching with heated KHF2 showed the best effect on strength and cement retention on zirconia with higher yttria content (>5 mol%). Application of KHF2 was, however, complicated on crown-shaped specimens. Pre-treatment and cementation protocols should be optimized for different dental zirconias to improve both strength and retention.

Shear bond strength of acid and laser conditioned enamel and dentine to composite resin restorations: An in vitro study.

OBJECTIVE: To compare the shear bond strength of enamel or dentin conditioned with either Er,Cr:YSGG (erbium, chromium: yttrium-scandium-gallium-garnet) laser or phosphoric acid to composite resin restoration. MATERIAL AND METHODS: Forty posterior human extracted teeth were used. After mesiodistal sectioning of the teeth crowns, the samples were randomly divided into two groups-in the first group (E), bonding was performed on the enamel after roughening and in the second group (D), the enamel was removed and bonding was performed on the dentin. These groups were further randomly divided into two subgroups according to the type of etching (n = 20 each). In the acid-etched groups (EA and DA), the surfaces were etched with 37% phosphoric acid. In the laser-conditioned groups (EL and DL), the surfaces were conditioned with Er,Cr:YSGG laser. Total-etch adhesive system was used to bond all the 80 specimens resin composite. The composite was vertically light-cured, and the specimens were subjected to a shear bond strength test. Modes of bond failure were determined with a stereomicroscope. RESULTS: The highest shear bond strength was observed for the DA group (16.25 ± 1.10 MPa, p < 0.0001), whereas the lowest was observed for the DL group (8.56 ± 0.67 MPa). The adhesive failure mode was the most frequently observed in all groups. CONCLUSIONS: The shear bond strength of composite resin bonded to enamel and dentin etched with phosphoric acid was higher than when conditioned with Er,Cr:YSGG laser. Thus, laser conditioning is not recommended.

Effect of airborne-particle abrasion of a titanium base abutment on the stability of the bonded interface and retention forces of crowns after artificial aging.

STATEMENT OF PROBLEM: Published data have shown that a mechanical surface treatment of titanium surfaces increases bonding potential. However, most of the studies are based on shear or tensile tests performed on flat-surfaced specimens and do not take into consideration the retention given by the titanium base (ti-base) axial walls and the thermomechanical loading seen in a clinical setting. PURPOSE: The purpose of this in vitro study was to evaluate the influence of different airborne-particle abrasion (APA) methods of the ti-base surface on the stability of the bonded interface and retention forces between these titanium bases and lithium disilicate crowns after thermomechanical aging. MATERIAL AND METHODS: Sixty internal connection implants (Conelog) were restored with lithium disilicate crowns and bonded to the corresponding ti-bases (Conelog). The ti-bases were divided into 4 groups (n=15), 3 experimental groups applying different APA methods, 30-µm silica-modified Al2O3 particles (CoJet) (30-SiO-AlO), 50-µm Al2O3 (Cobra Aluoxyd) (50-AlO), 110-µm silica-modified Al2O3 particles (Rocatec Plus) (110-SiO-AlO), and 1 control group (NoT). Ti-bases were airborne-particle abraded (10 seconds, 0.25 MPa at a 10-mm distance) under standardized conditions in a custom-made APA device. All crowns were cemented with a resin cement (Multilink Hybrid Abutment). After aging (1 200 000 cycles, 49 N, 1.67 Hz; 5 °C-55 °C, 120 seconds), all specimens were assessed for the presence of bond failures by optical microscopy (×50). The retention forces (N) were tested by using a pull-off test (0.5mm/min). Modes of failure were classified (Type 1, 2, or 3). An additional ti-base representing each group was prepared for surface roughness (µm) calculation (Ra, Rc, Rz) with a noncontact laser profilometer, and representative scanning electron microscope (SEM) images were recorded (×1000). Chi-squared tests were performed to analyze the bonded interface failure and modes of failure, and a Kruskal-Wallis test was selected to evaluate retention force values (α=.05). RESULTS: The percentages of bonding failure after aging were 73.3% (NoT), 40% (30-SiO-AlO), 6.7% (50-AlO), and 40% (110-SiO-AlO). The stability of the bonded interface was influenced by the APA method applied (P<.05). Mean ±standard deviation retention force values varied from 206.3 ±86.3 N (NoT) to 420 ±139.5 N (50-AlO), and the differences between these 2 groups were significant (P<.05). Modes of failure were predominantly Type 2 (30-SiO-AlO; 50-AlO; 110-SiO-AlO) and Type 3 (NoT). CONCLUSIONS: Airborne-particle abrasion of the titanium surface increased the bond stability and retention forces between the ti-base and the respective crown. The use of 50-µm Al2O3 provided the most stable bonded interface among the different treatments.

Evaluation of bond strength of resin cement to Er:YAG laser-etched enamel and dentin after cementation of ceramic discs.

The purpose of this study was to investigate the shear bond strength (SBS) of ceramic discs luted to differently etched enamel and dentin surfaces. Occlusal surfaces of 64 carious-free human molars and vestibule surfaces of 64 first maxillary incisors were ground to get flat superficial dentin and flattened enamel respectively. After generating 4 groups according to the surface etching method (37% orthophosphoric acid, Er:YAG laser-contact handpiece/scanning handpiece (1 or 2 times of scanning)), ceramic discs were luted to the surfaces with adhesive resin cement (Variolink N, Vivadent Ets., Schaan/Liechtenstein). After etching and cementation, thermocycling of 5000 cycles (Sd Mechatronik Gmbh, Feldkirchen-Westerham, Germany) and SBS test (Servopulser EHFFD1; Shimadzu, Kyoto, Japan) were performed respectively. The surface morphologies of 2 specimens, etched enamel and dentin, prepared for each group were examined with SEM analysis. Failure modes were determined under a USB digital microscope. Data were analyzed with one-way analysis of variance (ANOVA) and Tukey HSD test (α = 0.05). SBS values in dentin surfaces showed statistically significant differences (p < 0.05) among tested groups. The highest SBS among dentin groups was determined in the group which had 2 times etching by Er:YAG laser (11.42 MPa) by a scanning handpiece. No statistical differences were observed in the other dentin or enamel groups. Laser etching seems to be a viable alternative to acid etching on both enamel and dentin surfaces while double etching of dentin with a scanning handpiece can improve the adhesion.

Optical changes of human dentin after non-vital bleaching and effect of Er,Cr:YSGG laser on micro-shear bond strength of a self-etch and an etch-and-rinse adhesive system.

The aim was to evaluate the optical changes of bleached human dentin and the efficacy of Er,Cr:YSGG laser on micro-shear bond strength (µSBS) of two adhesive systems for immediate and delayed applications. Seventy-two human dentin specimens (1 mm) were obtained. Colour measurements of 30 specimens (control and bleaching groups) were made at baseline, after bleaching and a 7-day delay. Differences at colour (ΔE00), translucency (ΔTP00) and whiteness (ΔWID) were calculated by recorded data. Forty-two specimens were used to compare µSBS of a self-etch (Clearfil SE Bond [SE]) and an etch-and-rinse (Prime&Bond NT [PBNT]) adhesive to bleached dentin. Additional to a negative group, six groups were contemplated for each adhesive, considering the time of composite application (immediate, delayed) and whether additional surface treatment by laser (1 W, 2 W) or not. Colour and µSBS data were statistically analysed. For optical analysis, only ΔE00 and ΔWID calculated for the difference between baseline and bleaching were found significantly different for control and bleaching groups. Whiteness of bleached specimens was remarkably decreased after a 7-day delay. Despite immediate applications of SE showing lower µSBS than negative control, delayed applications showed no significant differences except that of the 2 W laser etching. For PBNT, laser etching increased µSBS for both of the immediate and delayed applications, and no significant difference was observed from negative control. Related with the preferred adhesive system, Er,Cr:YSGG laser etching can be an alternative for optimal bond strength of immediate restorations, but the clinicians should always keep in mind that perceived colour and whiteness will change by the passing time which can affect the shade match.

Effect of high concentration nano-hydroxyapatite serum on shear bond strength of metal brackets following three different enamel surface preparation methods: An in vitro study.

OBJECTIVE: White spot lesion (WSL) is one of the most important complications of fixed orthodontic treatment. Many methods have been studied to prevent this problem. This study is aimed to investigate the effect of high concentration nano-hydroxyapatite (nHAP) on shear bond strength (SBS) of metal brackets and Adhesive Remnant Index (ARI) score in different preparation methods. MATERIAL AND METHODS: Sixty human premolars, which were extracted for orthodontic reasons were included in this in vitro study. The teeth were randomly divided into 4 groups of 15 each: one control group and three nHAP groups. After applying nHAP for 2 to 3 minutes daily for 10 days, the groups 2 to 4 underwent sandblasting using 50µm aluminium oxide and 30 seconds etching, 60 and 30 seconds etching, respectively, and the brackets were then bonded to the teeth. After debonding, SBS and ARI scores were recorded. Data were analysed using the ANOVA test and posthoc test for pairwise comparisons. RESULTS: No significant difference was observed in SBS between the control group and the nHAP groups. The sandblasted teeth showed significantly higher SBS than the 30 seconds etching after nHAP application (P=0.02). The teeth etched for 60 seconds showed a significantly higher ARI score than the 30 seconds etched teeth with (P=0.003) or without (P<0.001) nHAP application. CONCLUSIONS: The use of nHAP before bracket bonding can be considered as a caries preventive method since it did not compromise the SBS. Sixty seconds etching is recommended for less likely damage to the enamel after debonding.

Effect of zirconia etching solution on the shear bond strength between zirconia and resin cement.

STATEMENT OF PROBLEM: The bond between resin cement and zirconia is essential to the long-term retention of a zirconia crown. However, it is unclear if the existing methods provide a long-term bond between resin cement and zirconia. PURPOSE: The purpose of this in vitro study was to evaluate the effects of a zirconia etching solution on the shear bond strength between zirconia and resin cement. MATERIAL AND METHODS: Sixty yttria-stabilized tetragonal zirconia polycrystal (Y-TZP) disks (Ø8×5 mm) were divided into 4 groups (n=15). Each group was then treated with 1 of the following methods: airborne-particle abraded with 50-µm Al2O3 (AA); etched with zirconia etching solution (ZES); airborne-particle abraded with 50-µm Al2O3 and then etched with ZES (AA-ZES); etched with ZES and then airborne-particle abraded with 50-µm Al2O3 (ZES-AA). Sixty composite resin cylinders (Ø2.3×2.4 mm) were luted to the zirconia disks with a self-adhesive resin cement under constant load and then light-polymerized for 40 seconds. Specimens were stored in a 37 °C incubator in distilled water for 24 hours and then thermocycled for 1000 cycles between 5 °C and 55 °C. A universal testing machine with a crosshead speed of 0.5 mm/min was used to measure the shear force (N). The shear bond strength (MPa) was then calculated. One-way ANOVA was used to compare the mean shear bond strength among the groups (α=.05). The failure mode was evaluated by using light microscopy at ×90 magnification and categorized as an adhesive, cohesive, or mixed failure. RESULTS: Mean ±standard deviation shear bond strength for AA, ZES, AA-ZES, and ZES-AA groups were 9.9 ±2.6, 8.9 ±2.9, 9.6 ±3.9, and 11.0 ±2.3 MPa, respectively. There was no significant difference among the treatment groups (P>.05). CONCLUSIONS: A zirconia etching solution did not significantly improve the shear bond strength between zirconia and resin cement compared with airborne-particle abrasion with Al2O3.

Influence of Khat Extract (Catha edulis) on corrosion resistance of Co-Cr dental alloys / Influência do extrato de Khat (Catha edulis) na resistência à corrosão de ligas dentais Co-Cr

Objective: The aim of this experimental study was to assess the effect of khat extract with different concentrations on the corrosion resistance of cobalt-chromium (Co-Cr) dental alloys used for removable denture. Material and Methods:The corrosion resistance of three Co-Cr alloys (Neobond II®, Kera 501® and PD Casta H®) was evaluated in artificial saliva in presence of three different concentrations of khat extracts. Fusayama-Meyer artificial saliva was used as a reference solution. The corrosion properties of the alloys were analyzed using potentiodynamic polarization, electrochemical impedance spectroscopy and surface analysis. The data was presented in means, standard deviations, and related figures. Comparison between the different concentrations was done using 1-way ANOVA test. The surface analysis was performed using scanning electron microscopy (SEM). Results: the results showed that the corrosion resistance of the three alloys tested (Neobond II®, Kera 501® and PD Casta H®) decreased in artificial saliva containing khat extract compared with that of the reference solution. Additionally, the corrosion resistance of the three Co-Cr dental alloys decreased by increasing the concentration of khat extract. Furthermore, the results indicate that Neobond II® alloy showed the least corrosion resistance compared with that of Kera 501® and PD Casta H® alloys. Conclusion: Khat extract with different concentrations had negative impact on the corrosion resistance of Cr-Co alloys. More in-vivo studies are highly recommended to confirm the results of the present study (AU)

Objetivo: O objetivo deste estudo experimental foi avaliar o efeito do extrato de khat em diferentes concentrações na resistência à corrosão de ligas dentárias de cobalto-cromo (Co-Cr) utilizadas em próteses removíveis. Material e Métodos:A resistência à corrosão de três ligas de Co-Cr (Neobond II®, Kera 501® e PD Casta H®) foi avaliada em saliva artificial na presença de três concentrações diferentes de extratos khat. A saliva artificial de Fusayama-Meyer foi usada como solução de referência. As propriedades de corrosão das ligas foram analisadas usando polarização potenciodinâmica, espectroscopia de impedância eletroquímica e análise de superfície. Os dados foram apresentados em médias, desvios-padrão e figuras relacionadas. A comparação entre as diferentes concentrações foi feita usando o teste One-way ANOVA. A análise de superfície foi realizada em microscopia eletrônica de varredura (MEV). Resultados: os resultados mostraram que a resistência à corrosão das três ligas testadas (Neobond II®, Kera 501® e PD Casta H®) diminuiu na saliva artificial contendo extrato khat em comparação com a solução de referência. Além disso, a resistência à corrosão das três ligas dentais Co-Cr diminuiu com o aumento da concentração de extrato de khat. Além disso, os resultados indicam que a liga Neobond II® apresentou a menor resistência à corrosão em comparação com as ligas Kera 501® e PD Casta H®. Conclusão: O extrato de Khat com diferentes concentrações teve impacto negativo na resistência à corrosão de ligas de Cr-Co. Mais estudos in vivo são altamente recomendados para confirmar os resultados do presente estudo. (AU)

Diferenciação oxidativa em dispositivos temporários de ancoragem de Ti6Al4V e aço 316L ­ estudo piloto / Oxidative differentiation in temporary anchoring devices made by Ti6Al4V and 316L steel ­ a pilot study

Resumo Este estudo piloto testou a hipótese de que os dispositivos temporários de ancoragem (DATs) fabricados de Aço 316L são mais resistentes à corrosão, mesmo em meio com flúor, do que os DATs fabricados a partir de ligas de titânio, para tanto foram realizadas medições eletroquímicas em Potenciostato. Materiais e Métodos: Quatro amostras de cada material foram testadas em cada conjunto de teste, a formulação artificial de saliva de Fusayama foi usada como eletrólito solução neste estudo de corrosão in vitro, sem flúor em sua composição e, em um segundo momento, com a concentração de 1500ppM de flúor em sua composição. No teste, uma polarização catódica foi então realizada aumentando essa voltagem por 5 minutos ou até que se obtivessem os pitins de corrosão. Em saliva artificial contendo até 1500ppmF- foi repetido esse teste com novas amostras de cada material em solução de saliva artificial sem a presença de flúor. Resultados: Os resultados de escala de corrente de indução foram inseridos no software OriginPro8 para confecção dos gráficos de valores. Tratando-se de um número reduzido de amostras, para não violar a confiabilidade do estudo, não se realizou teste estatístico. Dentre todas as ligas metálicas utilizadas atualmente, a liga de Ti6Al4V apresentou uma boa resistência à corrosão em saliva artificial. Entretanto a corrosão dessas ligas ocorre em contato com altas concentrações de flúor, diferentemente da liga de Aço 316L, que além da corrosão faz a passivação da superfície. (AU)

Abstract The aim of this pilot study was to test the hypothesis that temporary anchoring devices (TADs) made of 316L steel are more resistant to corrosion even in fluorine environment than DATs manufactured in addition to titanium alloys, for this Potentiostat electrochemical measurements were performed. Materials and Methods: Four pieces of each material were tested in each test set, an application of Fusayama artificial saliva was used as an electrolytic solution in this study of in vitro corrosion, without fluorine in its composition and in a second moment with 1500ppM of fluorine in its composition. In the test, a cathodic polarization was performed by increasing this voltage for 5 minutes or until the corrosion pins were obtained. In artificial saliva containing up to 1500ppmF- this test was repeated with new samples of each material in artificial saliva solution without fluorine. Results: The results of the induction current scale were inserted into OriginPro8 software for making value graphs. As there was a small number of samples, in order not to violate the study's reliability no statistical test was performed. Among all metal alloys currently used the Ti6Al4V alloy showed good resistance to corrosion in artificial saliva. However, the corrosion of these alloys occurs in contact with high fluorine concentration, unlike 316L steel alloy, which in addition to corrosion makes surface passivation. (AU)

How sandblasting on lingual surfaces can be carried out with minimum enamel damage: An in vitro study on human teeth.

OBJECTIVE: The aim was to assess the extent of enamel damage sandblasting might cause and to identify a combination of sandblasting durations and MicroEtcher nozzle-tooth surface distance (NTD) resulting in the least enamel damage. MATERIALS AND METHODS: Lingual surfaces of 30 human teeth were sandblasted with 2 different distances: 1, 2mm and 3 different durations: 1, 2, 3s and photographed using a light microscope. The cavity depth and diameter of the sandblasted teeth were measured on the light microscope's pictures. A pilot study was performed to minimize possible combinations of sandblasting durations and distances. To validate the measurement method, sandblasted teeth were ground cut for comparison. Inter-examiner reliability was assessed with Bland-Altman analysis. Mann-Whitney U-test was used to detect cavity and diameter changes for every sandblasting duration and NTD combination. RESULTS: From the pilot study sandblasting durations 1,2 and 3s and NTD<2mm were chosen. The cavity diameter of the sandblasted area did not change with increased sandblasting duration nor NTD (P>0.05). The cavity depth of the sandblasted area increased statistically with an increased sandblasting duration (P<0.05) but did not increase with an increase NTD (P>0.05). The 95% limits of inter-examiner agreement were narrow. CONCLUSION: All distance and duration combinations tested caused enamel damage. Sandblasting duration had greater impact on the cavity depth than the NTD. The blasting duration should, therefore, not exceed 2s and the NTD should be held at maximum 2mm to minimize the risk of unintentional spread.

[Research progress in surface bonding pretreatment of dental zirconia ceramics].

Yttria stabilized tetragonal zirconia polycrystal ceramics is widely used in the field of dentistry because of its excellent mechanical properties and biocompatibility. However, it has low hydroxyl content and does not contain silica. Therefore micro mechanical retention induced by hydrofluoric acid etching on its surface is not applicable. The bonding of zirconia is a difficult problem. Zirconia surface pretreatment is commonly used to improve bonding strength and durability. This review summarizes surface pretreatment of dental zirconia ceramic including air abrasion, laser etching, acid etching, silica coating, non-thermal plasmas treatment, et al. In addition, it presents advantages and disadvantages of each treatment, provides guidance for application and future research directions.

Resin-dentin bond stability of etch-and-rinse adhesive systems with different concentrations of MMP inhibitor GM1489.

Enzymatic degradation of the hybrid layer can be accelerated by the activation of dentin metalloproteinases (MMP) during the bonding procedure. MMP inhibitors may be used to contain this process. Objective To evaluate the degree of conversion (DC%), dentin bond strength (µTBS) (immediate and after 1 year of storage in water), and nanoleakage of an experimental (EXP) and a commercial (SB) adhesive system, containing different concentrations of the MMP inhibitor GM1489: 0, 1 µM, 5 µM and 10 µM. Methodology DC% was evaluated by FT-IR spectroscopy. Dentin bond strength was evaluated by µTBS test. Half of beams were submitted to the µTBS test after 24 h and the other half, after storage for 1 year. From each tooth and storage time, 2 beams were reserved for nanoleakage testing. Data were analyzed using ANOVA and Tukey's test to compare means (α=0.05). Results All adhesive systems maintained the µTBS after 1 year of storage. Groups with higher concentrations of inhibitor (5 µM and 10 µM) showed higher µTBS values than groups without inhibitor or with 1 µM. The nanoleakage values of all groups showed no increase after 1 year of storage and values were similar for SB and EXP groups, in both storage periods. The inhibitor did not affect the DC% of the EXP groups, but the SB5 and SB10 groups showed higher DC% values than those of SB0 and SB1. Conclusions The incorporation of GM1489 in the adhesive systems had no detrimental effect on DC%. The concentrations of 5 µM GM1489 for SB and 5 µM or 10 µM for EXP provided higher µTBS than groups without GM1489, in the evaluation after 1 year of storage; whereas the concentration of inhibitor did not affect adhesive systems nanoleakage.

Depth of acid penetration and enamel surface roughness associated with different methods of interproximal enamel reduction.

OBJECTIVES: To assess and compare the enamel surface quality after interproximal enamel reduction (IPR) was performed with different systems and to study the relation between acid penetration depth and enamel surface quality as well as the importance of remineralization. METHODS: Sixty-five extracted teeth were randomly allocated to five experimental groups: untreated control, manual with New Metal Strips, mechanical with oscillating segment (OS) discs, Safe-Tipped Bur Kit, and the Ortho-Strip, followed by 30 s of polishing with the Softflex system and the Compo-system after treating the tooth with OS discs. Mesial surfaces were demineralized for 24 h and distal surfaces were subjected to interchanging demineralization and remineralization cycles of 24 h each for 18 days. The analysis was carried out by profilometry, scanning electron microscopy, and polarization microscopy. RESULTS: After IPR and polishing, enamel roughness was reduced for all systems tested except for the Essix Safe-Tipped Bur Kit. Subsequent demineralization increased enamel roughness in all groups except controls beyond the original level prior to IPR except for IPR with New Metal Strips or Ortho-Strips and subsequent polishing. Cyclic demineralization and remineralization for 18 days yielded a reduction in acid penetration depth and an increase in surface smoothness, which correlated with each other only for controls and treatment with New Metal Strips or Ortho-Strips. CONCLUSIONS: Manual IPR, using New Metal Strips and, even more, the oscillating IPR system Ortho-Strips, yielded smoother interproximal enamel surfaces and less acid penetration depth than the IPR systems with OS discs and the Safe-Tipped Bur Kit after polishing and 18 days of cyclic demineralization and remineralization. Irrespective of the IPR procedure, proper remineralization of IPR-treated surfaces is advisable to reduce caries susceptibility.

The effect of diode laser application on restoration of non carious cervical lesion: Clinical follow up.

AIMS: The aim of this study is to evaluate the effect of the diode laser used for dentin sensitivity on the clinical success of non-carious cervical lesion (NCCL) restorations restored with different adhesive systems. METHODS: 20 NCCLs were restorated with Universal Single Bond (Self Etch) (3M, USA) and Grandio (Voco, Germany), 20 NCCLs were restorated with Universal Single Bond (Total Etch) and Grandio. After diode laser application, 20 NCCLs were restorated with Universal Single Bond and Grandio, 20 NCCLs were restorated with Universal Single Bond (Total Etch) and Grandio. The restorations were clinical evaluated by two examiners at baseline, for 6 and 18 months using modified United States Public Health Service (USPHS) Criteria. Chi-square test was used for statistical analyse. RESULTS: The lowest rates of retention was found in the Group 1. There was no statistically significant difference among the groups in marginal discoloration, marginal integrity, sensitivity (P > 0.05). CONCLUSION: Diode laser application prior to the restoration of teeth with NCCL don't reduce the retention rate of restorations, may reduce hypersensitivity and may affect the success of restoration. However, further laboratory and clinical studies are required.